HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178438829, compound → HCID 178438830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178438829 | HCID 178438829 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178438830 | HCID 178438830 | 86.9% |
Reaction Steps
A solution of 0.15 g (0.24 mmols) of 8 and 25 mg of Pd—C catalyst in 20 mL of anhydrous ethanol was subjected to hydrogenation conditions at 1 atm pressure for 2 h. The catalyst was filtered off and the crude product was reslurried in 98:2 mixture of diethylether:ethanol to afford 90 mg of the phosphate 9 as off white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120745B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-449d3097167e493c8c9a845c5c0fcd13 |
| Source note | uspto-grants-2015_09 |