HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 59355205, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | 2,7-bis(3,5-dimethylpiperidin-1-ylsulfonyl)-10-methylacridin-9(10H)-one | HCID 46851181 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 59355205 | HCID 59355205 | 86.8% |
Reaction Steps
A mixture of compound 11-4 (560 mg, 1 mmole), anhydrous toluene (10 mL) and Lawesson's reagent (820 mg, 2 mmole) was refluxed for 4 hrs. Toluene was removed by evaporation. To the residue methanol (20 mL) was added, stirred for few minutes at room temperature and the product was collected by filtration and dried to give 500 mg of the title compound. MS 576 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120754B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-5de99dc5db1e4000940e1ecbee64932d |
| Source note | uspto-grants-2015_09 |