HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(6-Bromo-4-chloroquinolin-3-yl)-3-methylbutan-1-one → HCID 178446972, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(6-Bromo-4-chloroquinolin-3-yl)-3-methylbutan-1-one | HCID 86692843 | — |
| Reactant | HCID 178419079 | HCID 178419079 | — |
| Product | HCID 178446972 | HCID 178446972 | 56% |
Reaction Steps
Following general procedure B, 1-(6-bromo-4-chloroquinolin-3-yl)-3-methylbutan-1-one (309 mg, 0.950 mmol) was reacted with tert-butyl trans-4-aminocyclohexylcarbamate (407 mg, 1.90 mmol) to afford the desired product (267 mg, 56%) as a yellow solid: ESI MS m/z 504 [C20H26BrN3O+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-4b4483c61e9b488ebdbfdc8faea4ab1d |
| Source note | uspto-grants-2015_09 |