HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(6-Bromo-4-chloroquinolin-3-yl)-3-methylbutan-1-one → HCID 178446971, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(6-Bromo-4-chloroquinolin-3-yl)-3-methylbutan-1-one | HCID 86692843 | — |
| Reactant | HCID 178484105 | HCID 178484105 | — |
| Product | HCID 178446971 | HCID 178446971 | 21.5% |
Reaction Steps
Following general procedure B, 1-(6-bromo-4-chloroquinolin-3-yl)-3-methylbutan-1-one (44 mg, 0.14 mmol) was reacted with trans-N1,N1-dimethylcyclohexane-1,4-diamine (92 mg, 0.43 mmol) to afford the desired product (13 mg, 21%) as an off-white solid: ESI MS m/z 433 [C22H30BrN3O+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-5166f659b25e40a6b57cc51613effa96 |
| Source note | uspto-grants-2015_09 |