HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-nitropyrimidine → HCID 86692877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-nitropyrimidine | HCID 82544 | — |
| Reactant | tert-butyl N-(pyrrolidin-3-yl)carbamate | HCID 2757234 | — |
| Product | HCID 86692877 | HCID 86692877 | 65.2% |
Reaction Steps
Following General procedure H, 2-chloro-5-nitropyrimidine (500 mg, 3.1 mmol) was reacted with tert-butyl pyrrolidin-3-ylcarbamate (632 mg, 3.5 mmol) followed by reduction to afford the desired product (565 mg, 65%) as a purple solid: ESI MS m/z 280 [C13H21N5O2+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-23368d3249434c129dff027aeca3b145 |
| Source note | uspto-grants-2015_09 |