HuagongsheHuagongshe Chemistry Print Report · For research reference only
N2-(2-(dimethylamino)ethyl)pyridine-2,5-diamine → HCID 66715402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N2-(2-(dimethylamino)ethyl)pyridine-2,5-diamine | HCID 16772731 | — |
| Reactant | 1-(6-Bromo-4-chloroquinolin-3-YL)ethanone | HCID 66715483 | — |
| Product | HCID 66715402 | HCID 66715402 | 74.7% |
Reaction Steps
Following General procedure C, 1-(6-bromo-4-chloroquinolin-3-yl)ethanone (284 mg, 1 mmol) was reacted with N2-(2-(dimethylamino)ethyl)pyridine-2,5-diamine (270 mg, 1.5 mmol) to afford the desired product (320 mg, 74%) as a yellow solid: ESI MS m/z 428 [C20H22BrN5O+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-b70f75912ef14df89d645b0a9b94ce92 |
| Source note | uspto-grants-2015_09 |