HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-(5-aminopyridin-2-yl)carbamate → HCID 66715959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-(5-aminopyridin-2-yl)carbamate | HCID 22064440 | — |
| Reactant | (6-Bromo-4-chloroquinolin-3-yl)(cyclopropyl)methanone | HCID 66715111 | — |
| Product | HCID 66715959 | HCID 66715959 | 72.8% |
Reaction Steps
Following General procedure C, (6-bromo-4-chloroquinolin-3-yl)(cyclopropyl)methanone (311 mg, 1 mmol) was reacted with tert-butyl 5-aminopyridin-2-ylcarbamate (313 mg, 1.5 mmol) to afford the desired product (352 mg, 72%) as a yellow solid: ESI MS m/z 483 [C23H23BrN4O3+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-2f2e0ef07eea4faeaab5549f0cb9c6f8 |
| Source note | uspto-grants-2015_09 |