HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-[(4-aminophenyl)methyl]carbamate → HCID 86692889, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-[(4-aminophenyl)methyl]carbamate | HCID 2756041 | — |
| Reactant | (6-Bromo-4-chloroquinolin-3-yl)(cyclopropyl)methanone | HCID 66715111 | — |
| Product | HCID 86692889 | HCID 86692889 | 78.1% |
Reaction Steps
Following general procedure C, (6-bromo-4-chloroquinolin-3-yl)(cyclopropyl)methanone (290 mg, 0.934 mmol) was reacted with tert-butyl 4-aminobenzylcarbamate (312 mg, 1.40 mmol) to afford the desired product (362 mg, 78%) as a yellow solid: ESI MS m/z 496 [C25H26BrN3O3+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-972ad3e6d3744a22abdc8b3fde2a55f3 |
| Source note | uspto-grants-2015_09 |