HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl 4-(5-aminopyridin-2-yl)piperazine-1-carboxylate → HCID 86692892, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl 4-(5-aminopyridin-2-yl)piperazine-1-carboxylate | HCID 17999304 | — |
| Reactant | HCID 68091885 | HCID 68091885 | — |
| Product | HCID 86692892 | HCID 86692892 | 69% |
Reaction Steps
Following general procedure C, 1-(6-bromo-4-chloroquinolin-3-yl)butan-1-one (360 mg, 1.15 mmol) was reacted with tert-butyl 4-(5-aminopyridin-2-yl)piperazine-1-carboxylate (480 mg, 1.73 mmol) to afford the desired product (440 mg, 69%) as an orange solid: ESI MS m/z 554 [C27H32BrN5O3+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-dd56cfde82674bdcb1996dc624266e83 |
| Source note | uspto-grants-2015_09 |