HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl alcohol, p-amino-alpha-((dimethylamino)methyl)- → HCID 86692894, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl alcohol, p-amino-alpha-((dimethylamino)methyl)- | HCID 54334 | — |
| Reactant | (6-Bromo-4-chloroquinolin-3-yl)(cyclopropyl)methanone | HCID 66715111 | — |
| Product | HCID 86692894 | HCID 86692894 | 53.5% |
Reaction Steps
Following general procedure C, (6-bromo-4-chloroquinolin-3-yl)(cyclopropyl)methanone (240 mg, 0.770 mmol) was reacted with 1-(4-aminophenyl)-2-(dimethylamino)ethanol (139 mg, 0.770 mmol) to afford the desired product (187 mg, 53%) as a yellow solid: ESI MS m/z 454 [C23H24BrN3O2+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-746ed678ec8346e480e826340a520686 |
| Source note | uspto-grants-2015_09 |