HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(6-Bromo-4-chloroquinolin-3-YL)ethanone → HCID 178467070, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(6-Bromo-4-chloroquinolin-3-YL)ethanone | HCID 66715483 | — |
| Reactant | HCID 178484108 | HCID 178484108 | — |
| Product | HCID 178467070 | HCID 178467070 | 18.3% |
Reaction Steps
Following general procedure C, 1-(6-bromo-4-chloroquinolin-3-yl)ethanone (250 mg, 0.880 mmol) was reacted with trans-N1,N1-dimethylcyclohexane-1,4-diamine hydrochloride (280 mg, 1.32 mmol) to afford the desired product (63 mg, 18%): ESI MS m/z 390 [C19H24BrN3O+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-cd519183e85c48dca60b64d5f10b400d |
| Source note | uspto-grants-2015_09 |