HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dichloro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol → HCID 178454012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dichloro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol | HCID 66716108 | — |
| Reactant | HCID 178454009 | HCID 178454009 | — |
| Product | HCID 178454012 | HCID 178454012 | 99.9% |
Reaction Steps
Following general procedure D, tert-butyl trans-4-[6-bromo-3-(cyclopropanecarbonyl)quinolin-4-ylamino]cyclohexylcarbamate (49 mg, 0.100 mmol) was reacted with 2,5-dichloro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol (85 mg, 0.300 mmol) to afford the crude product (57 mg) as a white solid: ESI MS m/z 570 [C30H33Cl2N3O4+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-bc751c44162d43c1a83cb224ae435617 |
| Source note | uspto-grants-2015_09 |