HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-6-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol → HCID 86692907, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-6-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol | HCID 17750230 | — |
| Reactant | HCID 66715770 | HCID 66715770 | — |
| Product | HCID 86692907 | HCID 86692907 | 135.9% |
Reaction Steps
Following general procedure F, tert-butyl 4-[6-bromo-3-(cyclopropanecarbonyl)quinolin-4-ylamino]adamantylcarbamate (57 mg, 0.100 mmol) was reacted with 2-chloro-6-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol (43 mg, 0.150 mmol) to afford the crude product (84 mg) as a brown oil: ESI MS m/z 619 [C35H40ClN3O5+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-9d05c6a1e9944713bf7a740a0c30209a |
| Source note | uspto-grants-2015_09 |