HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Difluoro-4-(3,3,4,4-tetramethylborolan-1-yl)phenol → HCID 178467125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Difluoro-4-(3,3,4,4-tetramethylborolan-1-yl)phenol | HCID 66716402 | — |
| Reactant | HCID 178467071 | HCID 178467071 | — |
| Product | HCID 178467125 | HCID 178467125 | 59% |
Reaction Steps
Following general procedure D, tert-butyl trans-4-(3-acetyl-6-bromoquinolin-4-ylamino)cyclohexylcarbamate (47 mg, 0.100 mmol) was reacted with 2,6-difluoro-4-(3,3,4,4-tetramethylborolan-1-yl)phenol (97 mg, 0.382 mmol) to afford the desired product (30 mg, 59%) as a yellow solid: ESI MS m/z 512 [C28H31F2N3O4+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-4bc8be69b97e47d5bebb947b51a62045 |
| Source note | uspto-grants-2015_09 |