HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-6-methoxy-4-(3,3,4,4-tetramethylborolan-1-yl)phenol → HCID 178487408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-6-methoxy-4-(3,3,4,4-tetramethylborolan-1-yl)phenol | HCID 66716174 | — |
| Reactant | HCID 178467071 | HCID 178467071 | — |
| Product | HCID 178487408 | HCID 178487408 | 65% |
Reaction Steps
Following general procedure D, tert-butyl trans-4-(3-acetyl-6-bromoquinolin-4-ylamino)cyclohexylcarbamate (56 mg, 0.200 mmol) was reacted with 2-chloro-6-methoxy-4-(3,3,4,4-tetramethylborolan-1-yl)phenol (47 mg, 0.100 mmol) to afford the desired product (35 mg, 65%) as a yellow solid: ESI MS m/z 541 [C29H34ClN3O5+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120749B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-1428b79d017640c4b370715d11d3b591 |
| Source note | uspto-grants-2015_09 |