HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86654091, compound → HCID 178519366, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86654091 | HCID 86654091 | — |
| Reactant | HCID 178524171 | HCID 178524171 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 178519366 | HCID 178519366 | 72% |
Reaction Steps
The title compound is prepared from 1H-benzoimidazole-5-carboxylic acid and cis-7,9-difluoro-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline following a procedure analogous to that described in Example 1. Yield: 72% of theory; TLC: rf=0.37 (silica gel, CH2Cl2/MeOH/32% aqueous NH3 90:10:1); Mass spectrum (ESI+): m/z=368 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120769B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-7d57152f5cc247bb98cc0046d962c2b0 |
| Source note | uspto-grants-2015_09 |