HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 178484411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 178524091 | HCID 178524091 | — |
| Product | HCID 178484411 | HCID 178484411 | 20% |
Reaction Steps
The title compound is prepared from cis-4-(1H-benzoimidazole-5-carbonyl)-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline-8-carboxylic acid and dimethylamine (2 mol/L in tetrahydrofuran) following a procedure analogous to that described in Example 1. Yield: 20% of theory; LC (method 1): tR=2.08 min; Mass spectrum (ESI+): m/z=403 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120769B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-2a5a945455d743c083eb3484860445b2 |
| Source note | uspto-grants-2015_09 |