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HRID2272064

反应详情

EQUATION

反应方程式

HRID 2272064 的结构方程式

REACTANTS

反应物

3
结构：CN(C)C(On1nnc2cccnc21)=[N+](C)C.F[P-](F)(F)(F)(F)F
HCID9886157

Methanaminium, N-((dimethylamino)(3H-1,2,3-triazolo(4,5-b)pyridin-3-yloxy)methylene)-N-methyl-, hexafluorophosphate(1-) (1:1)

C10H15F6N6OP

结构：c1ccc2c(c1)CC[C@@H]1NCCC[C@H]21
HCID12327022

(4aS,10bR)-1,2,3,4,4a,5,6,10b-Octahydrobenzo[f]quinoline

C13H17N

结构：Cn1c(=O)[nH]c2cc(C(=O)O)ccc21
HCID14424857

1-Methyl-2-oxo-2,3-dihydro-1H-benzimidazole-5-carboxylic acid

C9H8N2O3

PRODUCTS

生成物

1
结构：Cn1c(=O)[nH]c2cc(C(=O)N3CCC[C@@H]4c5ccccc5CC[C@@H]43)ccc21
HCID86654113

未命名化合物

收率 15%

PROCEDURE

实验过程

The title compound is prepared from 1-methyl-2-oxo-2,3-dihydro-1H-benzoimidazole-5-carboxylic acid and cis-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline following a procedure analogous to that described in Example 1 [2-(7-aza-1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate is used]. Yield: 15% of theory; LC (method 4): tR=1.92 min; Mass spectrum (ESI+): m/z=362 [M+H]+.