HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178497443, compound → HCID 178519368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178497443 | HCID 178497443 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 178519368 | HCID 178519368 | 46% |
Reaction Steps
The title compound is prepared from cis-4-(1H-benzoimidazole-5-carbonyl)-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline-10-carboxylic acid methyl ester following a procedure analogous to that described in Example 34. Yield: 46% of theory; TLC: rf=0.27 (silica gel, CH2Cl2/MeOH/32% aqueous NH3 90:10:1); Mass spectrum (ESI+): m/z=362 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120769B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-7aac6e6b7bbe4294af00766fc35647cc |
| Source note | uspto-grants-2015_09 |