1-Bromo-3-methoxypropane → HCID 86729750, compound

HRID 2272591Notes

Reaction equation

HRID 2272591 reaction equation
[C:1]([C:3]1[CH:19]=[CH:18][C:6]([C:7]([NH:9][CH2:10][CH2:11][CH2:12][C:13]([O:15]CC)=[O:14])=[O:8])=[CH:5][CH:4]=1)#[N:2].Br[CH2:21][CH2:22][CH2:23][O:24][CH3:25]>>[C:1]([C:3]1[CH:4]=[CH:5][C:6]([C:7]([N:9]([CH2:10][CH2:11][CH2:12][C:13]([OH:15])=[O:14])[CH2:21][CH2:22][CH2:23][O:24][CH3:25])=[O:8])=[CH:18][CH:19]=1)#[N:2]

Participants

3

Reactant 2

HCID 5245511-Bromo-3-methoxypropaneHCID 60637584HCID 60637584, compound

Product 1

HCID 86729750HCID 86729750, compound

Procedure

Using ethyl 4-(4-cyanobenzamido)butanoate and 1-bromo-3-methoxypropane, and by the reaction and purification in the same manner as in the method described in Step 2 of Example 28, 4-(4-cyano-N-(3-methoxypropyl)benzamido)butanoic acid was obtained.

Workup

  1. customby the reaction and purification in the same manner as in the method

Sources & evidence

ORD record
ord-a05b03e91735449ea91cb6463f8eecde
Source dataset
uspto-grants-2015_09
Patent number
US09120776B2

Reaction notes

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