Isopropylamine → HCID 123298831, compound

Participants

Reaction Steps

In an argon atmosphere, 4.24 g (20.7 mmol) of Si(iPrNCHCHNiPr)(H)Cl was dissolved in 20 mL of hexane and after adding 2.51 g (42.4 mmol) of isopropylamine, the mixture was stirred at room temperature for 3 hours. Insoluble matters produced were separated by filtration, and the solvent was removed by distillation from the filtrate under atmospheric pressure. The obtained residue was distilled under reduced pressure (distillation temperature: 75° C./3.7×102 Pa) to obtain 1,3-diisopropyl-2-isopropylamino-1,3-diaza-2-silacyclopent-4-ene (Si(iPrNCHCHNiPr)(H)NHiPr) as a colorless liquid (yielded amount: 4.10 g, yield: 87%).

Provenance & Evidence