Propylamine → HCID 123886175, compound

Participants

Reaction Steps

In an argon atmosphere, 5.90 g (25.4 mmol) of Si(tBuNCHCHNtBu)(H)Cl was dissolved in 40 mL of hexane and after adding 3.03 g (51.3 mmol) of propylamine, the mixture was stirred at room temperature for 3 hours. Insoluble matters produced were separated by filtration, and the solvent was removed by distillation from the filtrate under atmospheric pressure. The obtained residue was distilled under reduced pressure (distillation temperature: 92° C./3.5×102 Pa) to obtain 1,3-di-tert-butyl-2-propylamino-1,3-diaza-2-silacyclopent-4-ene (Si(tBuNCHCHNtBu)(H)NHPr) as a pale yellow liquid (yielded amount: 5.99 g, yield: 92%).

Provenance & Evidence