HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11733829, compound → HCID 67081833, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11733829 | HCID 11733829 | — |
| Reactant | HCID 11851868 | HCID 11851868 | — |
| Product | HCID 67081833 | HCID 67081833 | 27% |
Reaction Steps
By following the process described in Stage A of Example 8, Example 10 is prepared from (4-amino-3-methoxyphenyl)(8-hydroxyimidazo[1,5-a]pyridin-3-yl)-methanone (described in Patent Application WO2006097625) with 1,17-diiodo-3,6,9,12,15-pentaoxaheptadecane (Example R2). After purification by flash chromatography on silica gel (dichloromethane/acetone gradient=90/10 to 70/30), 0.93 g (27%) of a yellow powder is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120819B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-52fd9b2e33d24c5bbee1c0258a1fb235 |
| Source note | uspto-grants-2015_09 |