Diisopropyl Ether → HCID 57500356, compound

Participants

Reaction Steps

The mixture of 0.95 g (2.14 mmol) of methyl 2-amino-5-[(6-benzyloxy-1-methoxy-2-methylindolizin-3-yl)carbonyl]benzoate, 0.21 g (3.21 mmol) of ammonium formate and 0.19 g of palladium-on-charcoal at 10% in 12 ml of N,N-dimethylformamide is stirred for 4 hours at ambient temperature. It is then filtered and concentrated to dryness. The solid obtained is taken up with diisopropyl ether and then filtered, to give 0.64 g (85%) of a yellow powder.

Provenance & Evidence