HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Bis(2-iodoethoxy)ethane → 2,2'-[Ethane-1,2-diylbis(oxyethane-2,1-diyloxy-3,1-phenylene)]bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Bis(2-iodoethoxy)ethane | HCID 593436 | — |
| Reactant | 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol | HCID 2734623 | — |
| Product | 2,2'-[Ethane-1,2-diylbis(oxyethane-2,1-diyloxy-3,1-phenylene)]bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) | HCID 69074350 | — |
Reaction Steps
By following the process described in Example R65, Example R67 is prepared by dimerization of 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol with 1-iodo-2-[2-(2-iodoethoxy)ethoxy]ethane (Example R5). A white powder is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09120819B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-c42057fa83d64c838ce5c87ff3b64b8f |
| Source note | uspto-grants-2015_09 |