HRID2273598

反应详情

EQUATION

反应方程式

HRID 2273598 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Isopropylamine (3 mL) is added to a solution of 4-bromo-1-fluoro-2-nitrobenzene (700 mg, 3.18 mmol) in ethanol. The reaction may be stirred for an appropriate time at an appropriate temperature, such as room temperature for overnight and concentrated. The residue may be purified by any appropriate method such as Biotage column chromatography to give 4-bromo-N-isopropyl-2-nitroaniline (770 mg).

WORKUP

后处理

  1. customThe reaction
  2. concentrationconcentrated
  3. customThe residue may be purified by any appropriate method such as Biotage column chromatography