HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → N,N-bis(trimethylsilyl)perfluorooctaneamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Hexadecane | HCID 11006 | — |
| Reactant | 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctanamide | HCID 67919 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | N,N-bis(trimethylsilyl)perfluorooctaneamide | HCID 86615112 | — |
Reaction Steps
First, perfluorooctaneamide (CF3(CF2)7CONH2) (46 g) was dissolved in n-hexane (300 ml). Thereafter, trimethylchlorosilane (15 ml) was dropped gradually into the solution obtained above, in a dry nitrogen atmosphere. Then this was allowed to react for two hours while being stirred. After the reaction was completed, hexadecane contained in the reaction solution was removed with the evaporator. Thus, N,N-bis(trimethylsilyl)perfluorooctaneamide was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560301B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-297020bd8b424536ad1a50bc562a8510 |
| Source note | uspto-grants-2009_07 |