HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → Sulfinylperfluorooctaneamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | N,N-bis(trimethylsilyl)perfluorooctaneamide | HCID 86615112 | — |
| Product | Sulfinylperfluorooctaneamide | HCID 23161206 | — |
Reaction Steps
Next, thionyl chloride (SOCl2) 2.4 g was added gradually to N,N-bis(trimethylsilyl)perfluorooctaneamide 12 g in the dry nitrogen atmosphere, which was allowed to react for two hours while being stirred. Then this was distilled and thereby sulfinylperfluorooctaneamide was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560301B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-780d5624590a4ce0802a7cc83eceee8a |
| Source note | uspto-grants-2009_07 |