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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 227389Generated: October 30, 2026

Tetrahydrofuran → HCID 22033037, compound

https://huagongshe.com/reaction/227389

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTetrahydrofuranHCID 8028—
ReactantTriethylamineHCID 8471—
ReactantMethanesulfonyl chlorideHCID 31297—
Reactant1-Benzyloxy-1-butanolHCID 19866552—
ProductHCID 22033037HCID 22033037—

Reaction Steps

The 1-benzyloxy-1-butanol (Aldrich, 0.22 g, 1.2 mmol), triethylamine (0.56 mL, 4.1 mmol), and methanesulfonyl chloride (0.15 mL, 1.9 mmol) in 10 mL THF were processed as described in Example 1C to give the title compound that was used directly in the next reaction.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07560481B2
Source datasetuspto-grants-2009_07
ORD IDord-01ec4ccab9eb4909b61bf722dafeae4a
Source noteuspto-grants-2009_07