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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 227391Generated: October 31, 2026

Triethylamine → 4-(methylthio)butyl Methanesulfonate

https://huagongshe.com/reaction/227391

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantMethanesulfonyl chlorideHCID 31297—
Reactant4-(Methylthio)butanolHCID 519793—
SolventTetrahydrofuranHCID 8028—
Product4-(methylthio)butyl MethanesulfonateHCID 44627118—

Reaction Steps

The 4-(methylthio)-1-butanol (Aldrich, 0.15 g, 1.2 mmol), triethylamine (0.56 mL, 4.1 mmol), and methanesulfonyl chloride (0.15 mL, 1.9 mmol) in 10 mL THF were processed as described in Example 1C to give the title compound that was used directly in the next reaction.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07560481B2
Source datasetuspto-grants-2009_07
ORD IDord-e5eac1804e7946aead912d9c9abea9e5
Source noteuspto-grants-2009_07