HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 1,3-Dioxolan-4-ylmethyl methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1,3-Dioxolane-4-methanol | HCID 21618 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1,3-Dioxolan-4-ylmethyl methanesulfonate | HCID 87145518 | — |
Reaction Steps
The glycerol formal (Aldrich, 0.26 g, 2.5 mmol), triethylamine (1.1 mL, 8.3 mmol), and methanesulfonyl chloride (0.30 mL, 3.7 mmol) in 20 mL THF were processed as described in Example 1C to give the title compound that was used directly in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560481B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-8fa5e47351eb4d72a032b15200704450 |
| Source note | uspto-grants-2009_07 |