HCID 86731184, compound → HCID 178492737, compound

HRID 2273994Notes

Reaction equation

HRID 2273994 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[C:12]1[CH:13]=[N:14][NH:15][CH:16]=1)[C:6]([OH:8])=[O:7].[CH3:17]C1C(B2OC(C)(C)C(C)(C)O2)=CNN=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[C:12]1[C:16]([CH3:17])=[N:15][NH:14][CH:13]=1)[C:6]([OH:8])=[O:7]

Participants

3

Reactant 2

HCID 86731184HCID 86731184, compoundHCID 178434487HCID 178434487, compound

Product 1

HCID 178492737HCID 178492737, compound

Procedure

Intermediate 3 was synthesized by following a similar route to Intermediate 1 using 3-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole in step 1A. LCMS (ESI) m/z: 233.0 (M+H)+.

Sources & evidence

ORD record
ord-8f3c79432c1149e2bd806342118af7ce
Source dataset
uspto-grants-2015_09
Patent number
US09126944B2

Reaction notes

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