Methylhydrazine → HCID 86658797, compound

HRID 2274613Notes

Reaction equation

[CH3:1][NH:2][NH2:3].Br[C:5]([CH3:12])([CH3:11])[C:6]([O:8][CH2:9][CH3:10])=[O:7]>>[CH3:11][C:5]([N:2]([CH3:1])[NH2:3])([CH3:12])[C:6]([O:8][CH2:9][CH3:10])=[O:7]

Participants

Reactant 2

HCID 6061Methylhydrazine

HCID 11745Propanoic acid, 2-bromo-2-methyl-, ethyl ester

Product 1

HCID 86658797HCID 86658797, compoundYield 97%

Procedure

According to the procedure described in the synthesis method of Compound XIV-1, methylhydrazine (7.12 g, 150 mmol) was reacted with ethyl 2-bromo-2-methylpropanoate (19.51 g, 100 mmol) to obtain the title compound (15.54 g, 96%).

Sources & evidence

ORD record: ord-45b8bc9d0f684fcea569390cc33c6269
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09126981B2

Reaction notes

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