Benzyl isocyanate → HCID 67303618, compound

HRID 2274618Notes

Reaction equation

HRID 2274618 reaction equation
[CH3:1][C:2]([N:9]([CH3:11])[NH2:10])([CH3:8])[C:3]([O:5][CH2:6][CH3:7])=[O:4].[CH2:12]([N:19]=[C:20]=[O:21])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[CH2:12]([NH:19][C:20]([NH:10][N:9]([C:2]([CH3:1])([CH3:8])[C:3]([O:5][CH2:6][CH3:7])=[O:4])[CH3:11])=[O:21])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 76639Benzyl isocyanateHCID 86658797HCID 86658797, compound

Product 1

HCID 67303618HCID 67303618, compoundYield 57%

Procedure

According to the procedure described in the synthesis method of Compound V-1, ethyl 2-methyl-2-(1-methylhydrazinyl)propanoate (10.27 g, 77.8 mmol) was reacted with benzyl isocyanate (15.53 g, 116.7 mmol) to obtain the title compound (12.97 g, 57%).

Sources & evidence

ORD record
ord-08c199c271bb4bee815412728c4fd58f
Source dataset
uspto-grants-2015_09
Patent number
US09126981B2

Reaction notes

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