HuagongsheHuagongshe Chemistry Print Report · For research reference only
Quinoxaline-5-carbaldehyde → (S)-1,1-diethoxy-N-(quinoxalin-5-ylmethyl)propan-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Quinoxaline-5-carbaldehyde | HCID 582505 | — |
| Reactant | (2S)-1,1-Diethoxy-2-propanamine | HCID 12398111 | — |
| Product | (S)-1,1-diethoxy-N-(quinoxalin-5-ylmethyl)propan-2-amine | HCID 67075656 | 78.5% |
Reaction Steps
According to the procedure described in the synthesis method of Compound IX-6, (S)-1,1-diethoxypropan-2-amine (Compound XVIII-1) (1.57 g, 10.0 mmol) was reacted with quinoxaline-5-carbaldehyde (1.34 g, 8.5 mmol) to obtain the title compound (1.93 g, 78%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09126981B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-b5f6afd63d1041b191d05444cc01e469 |
| Source note | uspto-grants-2015_09 |