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HRID227471

反应详情

EQUATION

反应方程式

HRID 227471 的结构方程式

REACTANTS

反应物

4
结构：C1COCCN1
HCID8083

Morpholine

C4H9NO

结构：C1CSCCN1
HCID67164

Thiamorpholine

C4H9NS

结构：CCOC(=O)c1c(S(=O)(=O)Cl)c2cc(Cl)ccc2n1S(=O)(=O)c1ccccc1
HCID22401482

未命名化合物

结构：CCOC(=O)c1c(S(=O)(=O)Cl)c2cc(Br)ccc2n1S(=O)(=O)c1ccccc1
HCID86592455

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1[nH]c2ccc(Cl)cc2c1S(=O)(=O)N1CCSCC1
HCID68445271

未命名化合物

PROCEDURE

实验过程

The titled compound was prepared using the procedures described in Steps B and C of Example 2, replacing in Step B ethyl 5-bromo-3-(chlorosulfonyl)-1-(phenylsulfonyl)-1H-indole-2-carboxylate with ethyl 5-chloro-3-(chlorosulfonyl)-1-(phenylsulfonyl)-1H-indole-2-carboxylate, and morpholine with thiomorpholine. Proton NMR for the product was consistent with the titled compound. ESI+MS: 389.1 [M+H]+.

WORKUP

后处理

  1. customThe titled compound was prepared