HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 178420437, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 178527937 | HCID 178527937 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178420437 | HCID 178420437 | — |
Reaction Steps
1 (0.33 g, 1.5 mmol), TEA (0.209 mL, 1.5 mmol), benzyl bromide (0.178 mL, 1.5 mmol) were dissolved in 10 mL of EtOH and kept under reflux overnight. The solvent was removed and the remaining oil was purified by flash-chromatography on silica gel, applying a CHCl3/MeOH gradient.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09126987B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-8a83695c21e346589b0879930e3c0e7d |
| Source note | uspto-grants-2015_09 |