HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Bromopropyl)benzene → HCID 178420273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Bromopropyl)benzene | HCID 12503 | — |
| Reactant | HCID 178527937 | HCID 178527937 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178420273 | HCID 178420273 | — |
Reaction Steps
1 (0.33 g, 1.5 mmol), TEA (0.209 mL, 1.5 mmol), and phenylpropylbromide (0.228 mL, 1.5 mmol) were dissolved in 10 mL of EtOH and kept under reflux overnight. The solvent was removed and the remaining oil was purified by flash-chromatography on silica gel, applying a CHCl3/MeOH gradient.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09126987B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-f9d722b5fdbe4304adb6aa2385b0682a |
| Source note | uspto-grants-2015_09 |