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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 227475Generated: October 27, 2026

Morpholine → HCID 10316316, compound

https://huagongshe.com/reaction/227475

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMorpholineHCID 8083—
ReactantAzetidineHCID 10422—
Reactantethyl 5-chloro-3-(chlorosulfonyl)-1-(phenylsulfonyl)-1H-indole-2-carboxylateHCID 22401482—
Reactantethyl 3-(chlorosulfonyl)-5-bromo-1-(phenylsulfonyl)-1H-indole-2-carboxylateHCID 86592455—
ProductHCID 10316316HCID 10316316—

Reaction Steps

Following the procedures described in Steps D and E of Example 1, replacing in Step D ethyl 5-chloro-3-(chlorosulfonyl)-1-(phenylsulfonyl)-1H-indole-2-carboxylate with ethyl 5-bromo-3-(chlorosulfonyl)-1-(phenylsulfonyl)-1H-indole-2-carboxylate, and morpholine with azetidine, the title compound was obtained. HRMS (ES) exact mass calculated for C12H13BrN3O3S (M+H+): 357.9856. Found 357.9859.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07560546B2
Source datasetuspto-grants-2009_07
ORD IDord-8a2606eff6544ef28b1a59de979ed04e
Source noteuspto-grants-2009_07