化工社化工社 化学情報印刷レポート · 研究参考用
m-Chlorophenylhydrazine hydrochloride → 3-Chloro-8-methoxy-6,6-dimethyl-5,6-dihydrobenzo[b]carbazol-11-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | m-Chlorophenylhydrazine hydrochloride | HCID 75331 | — |
| 反応物 | 7-Methoxy-1,1-dimethyl-3,4-dihydronaphthalen-2(1H)-one | HCID 13011007 | — |
| 反応物 | 3-Bromo-8-methoxy-6,6-dimethyl-5,6-dihydrobenzo[b]carbazol-11-one | HCID 66834292 | — |
| 生成物 | 3-Chloro-8-methoxy-6,6-dimethyl-5,6-dihydrobenzo[b]carbazol-11-one | HCID 66834792 | — |
反応手順
Under the same conditions as the method for synthesizing Compound A3-1 and Compound A4, the title compound was prepared as a crude product from Compound A2 and (3-chlorophenyl)-hydrazine hydrochloric acid salt.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09126931B2 |
| 出典データセット | uspto-grants-2015_09 |
| ORD ID | ord-f69f940b46e14520b60bf0f0c894ca5a |
| 出典メモ | uspto-grants-2015_09 |