Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | 2,3,4-Trimethoxybenzaldehyde | HCID 75006 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Product | HCID 5376945 | HCID 5376945 | — |
Reaction Steps
2,3,4-trimethoxybenzaldehyde (20 g) was dissolved in nitromethane (50 ml). Ammonium acetate (8.25 g) was added, and the reaction was heated to 50° C. for 2 hrs. The solvents were evaporated in vacuo. The orange residue was partitioned between water and DCM. The organic layer was washed with brine, dried over Na2SO4 filtered and concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09127007B2 |
|---|
| Source dataset | uspto-grants-2015_09 |
|---|
| ORD ID | ord-7b43c4c3f2bc487e968d16d6c98987e1 |
|---|
| Source note | uspto-grants-2015_09 |
|---|
