HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → 1-Phenylaminocarbonyl-1,3-dicyclohexyl-O-(N-2-butylideneamino)-isourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | 1,3-Dicyclohexyl-O-(N-2-butylideneamino)-isourea | HCID 86664633 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-Phenylaminocarbonyl-1,3-dicyclohexyl-O-(N-2-butylideneamino)-isourea | HCID 86664641 | 99.9% |
Reaction Steps
To a solution of 1,3-dicyclohexyl-O—(N-2-butylideneamino)-isourea (Cmpd. 2) (2.93 g, 10 mmol) in dichloromethane (15 ml) is phenylisocyanate (1.19 g, 10 mmol). The mixture is stirred 1 h at room temperature and evaporated to afford 4.12 g of the title compound as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09127098B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-31a0477833de44acaafe934fc805a700 |
| Source note | uspto-grants-2015_09 |