Silane, trimethoxy-7-octenyl- → HCID 86715410, compound

HRID 2275505Notes

Reaction equation

HRID 2275505 reaction equation
[CH2:1]([Si:9]([O:14]C)([O:12]C)[O:10]C)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH:7]=[CH2:8]>C(O)(=O)C>[CH2:1]([Si:9]([OH:14])([OH:10])[OH:12])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH:7]=[CH2:8]

Participants

3

Reactant 1

HCID 104124Silane, trimethoxy-7-octenyl-

Product 1

HCID 86715410HCID 86715410, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

By changing the reaction condition, 1,3-di(7-octenyl)disiloxane-1,1,3,3-tetraol, a dimer of the octenylsilanetriol, can be synthesized as main product. 0.60 g (yield: 78%) of 1,3-di(7-octenyl)disiloxane-1,1,3,3-tetraol was obtained in the same manner by adding 1 mL of a 3 wt % acetic acid aqueous solution and 1.0 g of 7-octenyltrimethoxysilane and carrying out reaction. The structure of the product was identified by NMR spectroscopy.

Workup

  1. customreaction

Sources & evidence

ORD record
ord-80d45863c4fc41fc94399e5695672f61
Source dataset
uspto-grants-2015_09
Patent number
US09127167B2

Reaction notes

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