HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 66661927, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 19694419 | HCID 19694419 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 66661927 | HCID 66661927 | — |
Reaction Steps
A mixture of 2-[1-benzyl-4-(hydroxymethyl)pyrrolidin-3-yl]phenol (101.4 mg, 0.0003580 mol) and palladium (10% on carbon, 75 mg) in methanol (5.0 mL, 0.12 mol) was stirred under hydrogen (balloon) overnight. The mixture was filtered and the filtrate was concentrated. The residue was used in next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09126927B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-3196c31de4404b0984e01d6f8761ea06 |
| Source note | uspto-grants-2015_09 |