HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-methylbutane → 4-Bromo-1-isopentylpyridin-2(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-methylbutane | HCID 7891 | — |
| Reactant | 4-Benzyloxy-2(1H)-pyridone | HCID 3607724 | — |
| Reactant | 4-Bromo-1-(cyclopropylmethyl)pyridin-2(1H)-one | HCID 58554515 | — |
| Reactant | 1-(Cyclopropylmethyl)-4-hydroxypyridin-2(1H)-one | HCID 59497098 | — |
| Reactant | 4-hydroxy-1-(3-methylbutyl)-1H-pyridin-2-one | HCID 66885665 | — |
| Product | 4-Bromo-1-isopentylpyridin-2(1H)-one | HCID 59497090 | — |
Reaction Steps
Intermediate D7 was prepared following the same procedure implemented for the synthesis of D3, using 4-hydroxy-1-(3-methylbutyl)-1H-pyridin-2-one as starting material, which was prepared by the same method used for the synthesis of intermediate D2, by reaction of 4-benzyloxy-1H-pyridin-2-one with 1-bromo-3-methylbutane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09132122B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-c385339a03864c93877070eb0c59130f |
| Source note | uspto-grants-2015_09 |