HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 76657794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | 2-(Trifluoromethoxy)benzaldehyde | HCID 2777192 | — |
| Product | HCID 76657794 | HCID 76657794 | 94% |
Reaction Steps
In a similar manner as described in Preparation Example 1, by using 2-(trifluoromethoxy)benzaldehyde (38.03 g, 200.0 mmol), sodium hydroxide (12.00 g, 300.0 mmol) and hydrochloric acid hydroxylamine (16.6 g, 240 mmol), a white solid required compound (38.67 g, 188 mmol, 94%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09132126B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-b4c638b8e2fb46e1b22003ec5d9ab630 |
| Source note | uspto-grants-2015_09 |