HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 28812093, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 28473083 | HCID 28473083 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 28812093 | HCID 28812093 | 65% |
Reaction Steps
In a similar manner as described in Preparation Example 25, by using methanol (60 mL), methyl-5-amino-3-(2-chlorophenyl)isoxazol-4-carboxylate (6.0 g, 23.75 mmol) and 3% sodium hydroxide aqueous solution (60 mL), a white solid required compound (3.66 g, 15.33 mmol, 65%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09132126B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-9cfb23c244164dc39ba3cf9014bfedcf |
| Source note | uspto-grants-2015_09 |