HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-3-butenoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-bromobutyrate | HCID 21964551 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-3-butenoate | HCID 67274119 | — |
Reaction Steps
Add Triethylamine to a solution of Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-bromo-butyrate (Step E) in carbon tetrachloride. After stifling approximately for 4 hours, the mixture can be filtered through a pad of silica gel few times, and concentrate to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09133073B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-3d1af42e85b44707a32099c562e6fbe2 |
| Source note | uspto-grants-2015_09 |