Sodium Iodide → HCID 67296279, compound

Participants

Reaction Steps

4-Mercaptophenylboric acid 5.55 g (32.5 mmol) was dissolved in 80 mL of acetonitrile, followed by addition of potassium carbonate 6.73 g (48.7 mmol), sodium iodide 0.73 g (4.87 mmol) and ethyl bromoacetate 5.40 mL (8.13 g, 48.7 mmol), and the mixture was stirred for 18 hours at room temperature. The reaction solution was concentrated, followed by addition of water to the residue, and the residue was extracted with ethyl acetate, washed with saturated brine and dried over anhydrous magnesium sulfate. The solvent was concentrated to give the title compound 7.80 g (yield 100%).

Provenance & Evidence