40987-31-3 → HCID 90407658, compound

HRID 2277495Notes

Reaction equation

HRID 2277495 reaction equation
[NH:1]1[CH:5]=[C:4]([C:6]2[CH:11]=[C:10]([C:12]#[N:13])[CH:9]=[CH:8][N:7]=2)[N:3]=[CH:2]1.Cl[CH2:15][CH:16]1[O:21][CH2:20][CH2:19][N:18]([CH3:22])[CH2:17]1>>[CH3:22][N:18]1[CH2:19][CH2:20][O:21][CH:16]([CH2:15][N:1]2[CH:5]=[C:4]([C:6]3[CH:11]=[C:10]([C:12]#[N:13])[CH:9]=[CH:8][N:7]=3)[N:3]=[CH:2]2)[CH2:17]1

Participants

3

Reactant 2

HCID 4700310740987-31-3HCID 178510201HCID 178510201, compound

Product 1

HCID 90407658HCID 90407658, compound

Procedure

The title compound was prepared from 2-(1H-imidazol-4-yl)pyridine-4-carbonitrile and 2-(chloromethyl)-4-methylmorpholine according to the procedure for the preparation of Example 43, part A (heating to 120°). [M+H] Calc'd for C15H17N5O, 284. Found, 284.

Workup

  1. temperatureA (heating to 120°)

Sources & evidence

ORD record
ord-ba3826f68a214b70b4ab54fa8adf4da3
Source dataset
uspto-grants-2015_09
Patent number
US09133166B2

Reaction notes

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